10.46243/jst.2022.v7.i01.pp97-102 registered
A New Simple Validated RP-HPLC-PDA Analytical Method for Estimation of Aceclofenec in Active Pharmaceutical Ingredients and Bulk Drug Form Used as Anti-Anti-Inflammatory Drug
Resolves to https://www.jst.org.in/index.php/pub/article/view/596
Held by Longman Publishers (India) · prefix 10.46243 live · DOI address https://doi.org/10.46243/jst.2022.v7.i01.pp97-102
Registered 29 Sep 2026 via crossref · record version 2 · last change 29 Sep 2026, 11:59 PM · record sha256 c630fb7808e9baec…
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JournalArticle — an article in a journal · Digital · Visual · en
A New Simple Validated RP-HPLC-PDA Analytical Method for Estimation of Aceclofenec in Active Pharmaceutical Ingredients and Bulk Drug Form Used as Anti-Anti-Inflammatory Drug (PrincipalTitle)
Published 2022-05-22
Part of Journal of Science & Technology · ISSN 2456-5660 · volume 7 · issue Special 1 · pages 97–102
Agents
- Sachin S. Garad Sachin S. Garad (author)
- Longman Publishers (publisher)
Identifiers DOI 10.46243/jst.2022.v7.i01.pp97-102
Abstract
A simple, economical, user -friendly, precise, accurate, robust, rugged and linear analyt ical method developed and validated for estimation (Assay) of Aceclofenac in Active Pharmaceutical Ingredients or bulk drug form.Isocratic HPLC method developed, flow rate is 1.5 ml/min, and column used Hemochrom C18 Intsil (150mm X 4.6 mm X 5 µm), Column temperature used is 25ºC. Mobile phase used is made from 50 volume of buffer consist of 0.1 % orthophosphoric acid and 50 volumes of organic phase consist of 90% Acetonitrile. The UV detection wavelength is 275 nm. Linearity of the method was observed 50 µ g/ml to 150 µg/ml. The retention time of Aceclofenac is ≈ 6.0 minute. This method was validated as per ICH guideline. (1) This method is very user -friendly and can be used for estimation of Aceclofenac in Active Pharmaceutical Ingredients and Bulk drug for m because Analytical method validation of this method is successfully achieved in present study
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| Element | Value | In the record |
|---|---|---|
| DOI Name DOI name | 10.46243/jst.2022.v7.i01.pp97-102 | doi |
| Referent Type referentType | Creation | referent |
| Referent Sub-Type referentSubType | JournalArticle — an article in a journal | type |
| Referent Name(s) referentName(s) | A New Simple Validated RP-HPLC-PDA Analytical Method for Estimation of Aceclofenec in Active Pharmaceutical Ingredients and Bulk Drug Form Used as Anti-Anti-Inflammatory Drug (PrincipalTitle, en) | titles |
| Basic Metadata basicMetadata | author: Sachin S. Garad Sachin S. Garad publisher: Longman Publishers published: 2022-05-22 part of: Journal of Science & Technology · ISSN 2456-5660 · vol. 7 · no. Special 1 · pp. 97–102 language: en form: Digital · Visual · Language | agents, dates, container, language, structural_type, modes, characters |
| Referent Identifier(s) alternateIdentifier(s) | none besides the DOI | identifiers, relations (IsSameAs) |
| Registration Authority registrationAuthorityCode | Crossref — issued by Crossref (member 25296); held here as a copy | record.source_agency (our code, ra_doi_name, for names issued here once appointed) |
| Created Date issueDate | 2024-02-16 | record.registered (when the DOI name was first registered) |
| relatedIdentifiers | none needed — the descriptive metadata is in this record | container, relations (only where the descriptive metadata lives at another identifier) |
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Every change to this DOI, in order, as it was recorded. Entries are only ever added, never changed or removed.
| # | When | What | By | Changes |
|---|---|---|---|---|
| 1 | 29 Sep 2026, 10:00 PM | register registered at Crossref; record read from api.crossref.org | Administrator (admin) | 73 fields set · sha256 366e73c3d7b4… |
| 2 | 29 Sep 2026, 11:59 PM | update record re-read from api.crossref.org | Administrator (admin) | container.titles.0.value: |
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